Relación de Métodos y alcance. de la Acreditación ante INDECOPI - SNA. Servicios Analíticos Generales S.A.C. Registro Nº LE-047

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1 Servicios Analíticos Generales S.A.C. Registro Nº LE-047 Servicio Nacional de Acreditación INDECOPI NTP - ISO / IEC 17025:2006

2 01 Aceites y grasas EPA-821-R Method 1664, 2010 (HEM Revision B. N-Hexane Extractable Material (HEM; Oil and Grease and Silica Gel Treated N-Hexane Extractable Material (SGT-HEM; Non-polar Material by Extraction and Gravimetry. Alcalinidad 02 (Carbonato, SM Part 2320-B, Bicarbonato y OH - Alkalinity. Titration Method. 03 Cianuro Libre SM Part 4500-CN J,E 04 Cianuro Total SM Part 4500-CN C,E, 05 Cianuro WAD SM Part 4500-CN I, E, Cyanide. Cyanogen Chloride. Cyanide. Total Cyanide after Distillation. Cyanide. Weak Acid Dissociable Cyanide. 06 Cloruros SM Part 4500-Cl B, Chloride. Argentometric Method. 07 Conductividad SM Part 2510 B, Conductivity. Laboratory Method. 08 Cromo VI SM Part 3500-Cr B, 22nd Edition / EPA-SW-846 Method 7196A, Revision 1 / 1992 Chromium Hexavalent (Colorimetric. Demanda Bioquímica 09 de Oxígeno (DBO SM Part 5210 B, 5 Biochemical Oxygen Demand (BOD. 5-Day BOD Test. Demanda Química 10 de Oxígeno SM Part 5220 D, (DQO Chemical Oxigen Demand (COD. Closed Reflux, 11 Dureza Cálcica o Calcio SM Part 3500-Ca B, 12 Dureza Total SM Part 2340 C, 13 Fenoles EPA-SW-846, Method Calcium. EDTA Titrimetric Method. Hardness. EDTA Titrimetric Method. Phenolics (Spectrophotometric Manual 4-AAP with distillation. SM: Standard Methods for the Examination of Water and Wastewater-APHA-AWWA-WEF. Página 1 de 5

3 14 Fluoruros SM Part 4500-F B, D, Fluoride. SPADNS Method. Aguas de Mar, Fósforo Total o Fósforo (P 15 SM Part 4500-P E, Fosfatos ( PO 4-3 EPA-821-R Method Hidrocarburos Totales 2010 Revision B. 17 Magnesio (Mg SM Part 3500-Mg B, 18 Nitratos SM Part 4500-NO3 B, 19 Nitratos SM Part 4500-NO3 E, Phosphorus. Ascorbic Acid Method. N-Hexane Extractable Material (HEM; Oil and Grease and Silica Gel Treated N-Hexane Extractable Material (SGT-HEM; Non-polar Material by Extraction and Gravimetry. Magnesium. Calculation Method Nitrogen (Nitrate. Ultraviolet Spectrophotometric Screening Method. Nitrogen (Nitrate. Cadmium Reduction Method. Agua Subterránea. 20 Nitritos SM Part 4500-NO 2 B, Nitrogen (Nitrite. 21 Nitrógeno Amoniacal SM Part 4500-NH 3 B, C, Nitrogen (Ammonia. Preliminary Distillation Step. Titrimetric Method. 22 Nitrógeno Amoniacal SM Part 4500-NH 3 D, Nitrogen Ammonia - Selective Electrode Method. Agua de Mar. Nitrógeno Total 23 SM Part 4500-Norg B, Nitrógeno Orgánico 24 Oxígeno Disuelto (OD SM Part 4500-O C, Nitrogen (Organic. Macro-Kjeldahl Method. Oxygen (Dissolved. Azide Modification. 25 ph SM Part 4500-H + B, ph Value. Electrometric Method. 26 S.A.A.M. (Detergentes SM Part 5540 C, Surfactans. Anionic Surfactants as MBAS. 27 Sólidos Disueltos Totales (TDS SM Part 2540 C, Solids. Total Dissolved Solids Dried at 180 C SM: Standard Methods for the Examination of Water and Wastewater-APHA-AWWA-WEF. Página 2 de 5

4 Sólidos 28 SM Part 2540 F, Sedimentales (SS Solids. Settleable Solids. Sólidos Suspendidos 29 SM Part 2540 D, Totales (TSS 30 Sólidos Totales (TS SM Part 2540 B, 31 Sulfatos SM Part 4500-SO 42 E, 32 Sulfuros SM Part 4500-S 2 D, 33 Sulfuros SM Part 4500-S 2 F, 34 Turbiedad SM Part 2130 B, PARÁMETROS INSTRUMENTALES ACREDITADOS Hidrocarburos Totales 35 de Petróleo EPA Method 8015 C, Revision (TPH 36 Metales Totales y Disueltos (Aluminio, Antimonio, Arsénico, Bario, Berilio, Boro, Cadmio, Calcio, Cerio, Cromo, Cobalto, Cobre, Hierro, Plomo, EPA-Method 200.7, Revision 4.4 Litio, Magnesio, Manganeso, EMMC Version. Mercurio, Molibdeno, Níquel, Fósforo, Potasio, Selenio, Silice (SiO 2, Plata, Sodio, Estroncio, Talio, Estaño, Titanio, Vanadio, Zinc 1994 PARÁMETROS MICROBIOLÓGICOS ACREDITADOS 37 Detección de Salmonella sp. SM Part 9260 B, (item 2.d., Solids. Total Suspended Solids Dried at C. Solids. Total Solids Dried at C. Sulfate. Turbidimetric Method. Sulfide. Methylene Blue Method. Sulfide. Iodometric Method Turbidity. Nephelometric Method. Nonhalogenated Organics by Gas Chromatography Determination of Metals and Trace Elements in water and wastes by Inductively Coupled Plasma-Atomic Emission Spectrometry Detection of Pathogenic Bacteria. Salmonella. Efluente doméstico, Efluente Industrial, Agua de Piscina, Agua de Mar. Efluente Industrial, Agua de Mar. Efluente Industrial, Agua de Mar. Agua de Mar, 38 Filtración de Membrana para Coliformes Fecales SM Part 9222 D, Membrane Filter Technique for Members of the Coliform Group. Thermotolerant (Fecal Coliform Membrane Filter Procedure. 39 Filtración de Membrana para Coliformes Totales SM Part 9222 B, Membrane Filter Technique for Members of the Coliform Group. Standard Total Coliform Membrane Filter Procedure. Agua de Mar, 40 Filtración de Membrana para Estreptococos Fecales y Enterococos SM Part 9230 C, (item 3.c., Fecal Enterococcus / Streptococcus Groups. Membrane Filter Techniques. Agua de Mar, SM: Standard Methods for the Examination of Water and Wastewater-APHA-AWWA-WEF. Página 3 de 5

5 PARÁMETROS MICROBIOLÓGICOS ACREDITADOS 41 Coliformes Fecales SM Part 9221 E, Multiple-Tube Fermentation Technique for Members of the Coliform Group. Fecal Coliform Procedure. 42 Coliformes Totales SM Part 9221 B, Multiple-Tube Fermentation Technique for Members of the Coliform Group. Standard Total Coliform Fermentation Technique. Agua de Mar, 43 Escherichia coli SM Part 9221 G (item 2, Multiple-Tube Fermentation Technique for Members of the Coliform Group. Other Escherichia coli Procedure (PROPOSED. Agua de Mar, 44 Estreptococos Fecales SM Part 9230 B, y Enterococos Fecales Fecal Enterococcus/Streptococcus Groups. Multiple-Tube Technique. Agua de Mar, 45 Recuento de Bacterias Heterotróficas por filtración SM Part 9215 D, Heterotrophic Plate Count. Membrane Filter Method. 46 Recuento de Bacterias Heterotróficas por incorporación SM Part 9215 B, Heterotrophic Plate Count. Pour Plate Method. 47 Vibrio cholerae SM Part 9260 H (Item 3.d.1, Detection of Pathogenic Bacteria. Vibrio. Agua de Mar, PARÁMETROS HIDROBIOLÓGICOS ACREDITADOS 48 Fitoplancton SM Part F (items: F.2.a, F.2.b y F.2.c.1, Plankton. Phytoplankton Counting Techniques Agua de Mar, Agua de Lago, Agua Estuarina, Agua de Laguna, Agua de Río. Macrobentos o 49 Macroinvertebrados SM Part C.2, Bentónicos Benthic Macroinvertebrates. Sample Processing and Analysis. Sedimento Marino, Sedimento Estuarino, Sedimento Epicontinental. 50 Perifiton SM Part C (ítems 1y 2, Periphyton. Sample Analysis. Sedgwick-Rafter Counts Inverted Microscope Method Counts. Agua de Lago, Agua de Laguna, Agua de Río. 51 Zooplancton SM Part G, Plankton. Zooplankton Counting Techniques. Agua de Mar, Agua Estuarina, Agua de Lago, Agua de Laguna, Agua de Río. 52 Aceites y grasas EPA SW-846 Method 9071 B N-Hexane Extractable Material (HEM for sludge, sediment, and solid samples. Lodos, Sedimentos, Suelos. 53 Conductividad ISO 11265:1994 / Cor1: Soil quality - Determination of the specific electrical conductivity. Sedimentos, Suelos. SM: Standard Methods for the Examination of Water and Wastewater-APHA-AWWA-WEF. Página 4 de 5

6 EPA-821-R Hidrocarburos Totales 2010 Method 1664 Revision B. N-Hexane Extractable Material (HEM; Oil and Grease and Silica Gel Treated N-Hexane Extractable Material (SGT-HEM; Non-polar Material by Extraction and Gravimetry. Sedimentos, Suelos. EPA-SW-846, Method 9045 D, 55 ph 2004 Soil and Waste ph. Lodos, Sedimentos, Suelos. Revision 4. PARÁMETROS INSTRUMENTALES ACREDITADOS Hidrocarburos Totales 56 EPA Method 8015 C, Revision de Petróleo (TPH METALES (Aluminio, Antimonio, Arsénico, Bario, Berilio, Boro, Cadmio, Calcio, 57 Cerio, Cromo, Cobalto, Cobre, Hierro, EPA-Method 200.7, Plomo, Litio, Magnesio, Manganeso, Revision 4.4 EMMC Version. Mercurio, Molibdeno, Níquel, Fósforo, 1994 Potasio, Selenio, Silice (SiO 2, Plata, Sodio, Estroncio, Talio, Estaño, Titanio, Vanadio, Zinc Nonhalogenated Organics by Gas Chromatography Determination of Metals and Trace Elements in water and wastes by Inductively Coupled Plasma-Atomic Emission Spectrometry Lodos, Sedimentos, Suelos. Lodos, Sedimentos, Suelos. Material Particulado 58 PM10 NTP (Alto Volumen 59 Dióxido de Azufre (SO EPA-40 CFR, Appendix A-2 to Part 50 Dióxido de Nitrógeno 60 (NO ASTM D Sulfuro de Hidrógeno (H 2 S SAG-16 / Referenciado en Norma COVENIN / Metales EPA Compendium Method IO Material Particulado EPA-40 CFR, Appendix A-3 to en Emisiones Part 60. Test Method 5. Dióxido de Azufre (SO EPA 40 CFR, Appendix A-4 to en Emisiones Part 60, Method 6. Método de referencia para la determinación de material particulado respirable como PM10 en la atmósfera. Determination of Sulfur Dioxide in the Atmosphere (Pararosaniline Method Standard Test Method for Nitrogen Dioxide content of the Atmosphere (Griess Saltzman-Reaction. Calidad de Aire Determination of Metals in Ambient Particulate Matter Using Inductively Coupled Plasma (ICP Spectroscopy Determination of Particulate Matter Emissions from Stationary Sources. Determination of Sulfur Dioxide Emissions from Stationary Sources. Emisiones. Emisiones. 65 Conductividad 66 Oxígeno Disuelto 67 ph SM Part 2510 B, SM Part 4500-O G, SM Part 4500-H + B, Conductivity. Laboratory Method Oxygen (Dissolved Membrane Electrode Method ph Value, Electrometric Method. Agua de Lluvia, Municipal (tratada y no tratada, Agua de Lluvia, Municipal (tratada y no tratada, Agua de Lluvia, Municipal (tratada y no tratada, 68 Temperatura SM Part 2550 B, Temperature. Laboratory and Field Methods. Agua de Lluvia, Municipal (tratada y no tratada, SM: Standard Methods for the Examination of Water and Wastewater-APHA-AWWA-WEF. Página 5 de 5

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